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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1459615Generated: October 30, 2026

Picolyl chloride → HCID 53710724, compound

https://huagongshe.com/reaction/1459615

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPicolyl chlorideHCID 23393—
Reactant2-[2-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]ethyl]-2H-1,4-benzoxazin-3(4H)-oneHCID 12048020—
ProductHCID 53710724HCID 53710724—

Reaction Steps

2-(2-tert-Butyldimethylsiloxyethyl)-3,4-dihydro-3-oxo-2H-1,4-benzoxazine was alkylated with 2-chloromethylpyridine by method F and the crude product was deprotected by method H without purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05854242
Source datasetuspto-grants-1998_12
ORD IDord-e15dafafb6584a9c96dd07cceff4e65e
Source noteuspto-grants-1998_12