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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1459618Generated: October 29, 2026

alpha-Chloro-m-nitrotoluene → HCID 54348374, compound

https://huagongshe.com/reaction/1459618

Reaction equation

Participants

RoleNameHCIDCharge
Reactantalpha-Chloro-m-nitrotolueneHCID 12078—
Reactant2-[2-[[(1,1-Dimethylethyl)dimethylsilyl]oxy]ethyl]-2H-1,4-benzoxazin-3(4H)-oneHCID 12048020—
ProductHCID 54348374HCID 54348374—

Reaction Steps

The intermediate silyl protected alcohol was prepared from 2-(2-tert-butyldimethylsiloxyethyl)-3,4-dihydro-3-oxo-2H-1,4-benzoxazine by Method F, alkylating with 3-nitrobenzyl chloride. Deprotection to the indicated product was carried out by method I.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05854242
Source datasetuspto-grants-1998_12
ORD IDord-ae13731806f24f4791b64173bae6c06e
Source noteuspto-grants-1998_12