4-Nitrobenzenesulfonyl chloride → HCID 54336054, compound

HRID 1459674Notes

Reaction equation

HRID 1459674 reaction equation
[N+:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10](Cl)(=[O:12])=[O:11])=[CH:6][CH:5]=1)([O-])=O.[NH2:14][C:15]1[C:28]2[NH:27][C:26]3[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=3)[S:20][C:19]=2[CH:18]=[CH:17][CH:16]=1>[C].[Pd]>[NH2:1][C:4]1[CH:9]=[CH:8][C:7]([S:10]([NH:14][C:15]2[C:28]3[NH:27][C:26]4[C:21](=[CH:22][CH:23]=[CH:24][CH:25]=4)[S:20][C:19]=3[CH:18]=[CH:17][CH:16]=2)(=[O:12])=[O:11])=[CH:6][CH:5]=1

Participants

4

Reactant 2

HCID 74044-Nitrobenzenesulfonyl chlorideHCID 15556090HCID 15556090, compound

Product 1

HCID 54336054HCID 54336054, compound

Reagents, catalysts & solvents 1

HCID 178418390HCID 178418390, compoundCatalyst

Procedure

4-Nitrobenzenesulfonyl chloride was reacted with 1-amino-10H-phenothiazine in the same manner as the one of Example 11. The product thus obtained was hydrogenated in the presence of palladium-carbon at room temperature under atmospheric pressure. Thus the title compound was obtained.

Workup

  1. customThe product thus obtained

Sources & evidence

ORD record
ord-22e62aaa97af41bc8aea0bc9ffe1a968
Source dataset
uspto-grants-1998_12
Patent number
US05854274

Reaction notes

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