Ether hydrochloride → HCID 19388492, compound

Participants

Reaction Steps

In 1 ml of chloroform was dissolved 0.5 g of methyl 4-(3,4-dimethoxy-2-hydroxybenzyl)-1-piperazinecarbodithioate. To the solution was dropwise added under chilling with ice 1.46 ml of 1-N HCl/ether mixture, and the resulting mixture was stirred at room temperature. Precipitated crystals were collected by filtration and washed with 6 ml of ether to give 0.53 g of the desired compound as a white powder, m.p. 204°-205° C. (decomp.), yield 95.9%.

Provenance & Evidence