Veratraldehyde → HCID 10543580, compound

HRID 1460207Notes

Reaction equation

HRID 1460207 reaction equation
[CH3:1][O:2][CH:3]([O:11][CH3:12])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1Br.[CH3:13][O:14][C:15]1[CH:16]=[C:17]([CH:20]=[CH:21][C:22]=1[O:23][CH3:24])[CH:18]=[O:19]>>[CH3:1][O:2][CH:3]([O:11][CH3:12])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][C:5]=1[CH:18]([OH:19])[C:17]1[CH:20]=[CH:21][C:22]([O:23][CH3:24])=[C:15]([O:14][CH3:13])[CH:16]=1

Participants

3

Reactant 2

HCID 8419VeratraldehydeHCID 111489431-Bromo-2-(dimethoxymethyl)benzene

Product 1

HCID 10543580HCID 10543580, compoundYield 89%

Procedure

2-bromobenzaldehyde dimethylacetal and 3,4-dimethoxybenzaldehyde are reacted in the same manner as described in Example 1-(1), whereby 2-(3,4-dimethoxy-α-hydroxybenzyl)benzaldehyde dimethylacetal is obtained as pale yellow syrup.

Sources & evidence

ORD record
ord-207c359cdc1043819b46424a88efd4d5
Source dataset
uspto-grants-1991_12
Patent number
US05070103

Reaction notes

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