HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14877952, compound → HCID 14877953, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14877952 | HCID 14877952 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 14877953 | HCID 14877953 | 56% |
Reaction Steps
Following the general procedure of Example 6, 0.21 g (0.67 mmole) of 3,3-bis(4-fluorophenyl)-2-(1H-tetrazol-1-yl)-2-propenol was treated with 288 mg (1.33 mmoles) of pyridinium chlorochromate in 10 mL of methylene chloride and there was thereby produced 117 mg (56%) of the title compound after crystallization from ethyl acetate-hexanes; m.p. 160.7°-161.4° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05070206 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-caca07b3e3134dc397f8010127993749 |
| Source note | uspto-grants-1991_12 |