Dichloromethane → HCID 14324551, compound

Participants

Reaction Steps

To a mixture of 800 g of 3-nitro-4-chlorobenzenesulfonyl chloride and 1,000 ml of dichloromethane, was added dropwise a dichloromethane solution containing 600 g of hexadecylamine and 251 ml of triethylamine. After completion of the reaction, the reaction solvent was removed by distillation under reduced pressure. The residue was dissolved in 3,000 ml of methanol under heating, followed by gradually cooling to precipitate crystals, which were collected by filtration and dried to give 1,020 g (88%) of the noted compound.

Provenance & Evidence