Methanol → HCID 131717093, compound

HRID 1460593Notes

Reaction equation

HRID 1460593 reaction equation
[N:1]([C:4]12[CH2:13][CH2:12][CH2:11][CH2:10][CH:9]1[CH2:8][O:7][C:6]1[CH:14]=[CH:15][CH:16]=[CH:17][C:5]2=1)=[C:2]=[O:3].[CH3:18][OH:19]>>[CH3:18][O:19][C:2](=[O:3])[NH:1][C:4]12[CH2:13][CH2:12][CH2:11][CH2:10][CH:9]1[CH2:8][O:7][C:6]1[CH:14]=[CH:15][CH:16]=[CH:17][C:5]2=1

Participants

3

Reactant 2

HCID 887MethanolHCID 19107030HCID 19107030, compound

Product 1

HCID 131717093HCID 131717093, compound

Procedure

A solution of the product from Example 71 (0.66 g, 2.88 mmol) in 20 ml methanol was refluxed 18 hours. Evaporation and chromatography gave the title compound (0.75 g).

Workup

  1. customEvaporation and chromatography

Sources & evidence

ORD record
ord-20a8a7af15e94ee3ae47cd18df2567d6
Source dataset
uspto-grants-1991_12
Patent number
US05071853

Reaction notes

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