HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-2-nitroaniline → 2-Bromo-4-chloro-6-nitrobenzenamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-2-nitroaniline | HCID 6979 | — |
| Reactant | Bromine | HCID 24408 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 2-Bromo-4-chloro-6-nitrobenzenamine | HCID 11064884 | 81% |
Reaction Steps
In glacial acetic acid, 51.8 g (300 mmoles) of 4-chloro-2-nitroaniline was reacted with 57.5 g (360 mmoles) of bromine to give 61.6 g (243 mmoles) of 6-bromo-4-chloro-2-nitroaniline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05071995 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-2ade098f3c134d7ab47d072ce9466e48 |
| Source note | uspto-grants-1991_12 |