HRID1460773

反应详情

EQUATION

反应方程式

HRID 1460773 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

10.3 g (50 mmol) of ethyl N-(2-chloroallyl)-N-(2 -oxoethyl)-carbamate are heated under reflux overnight with 5.2 g (50.5 mmol) of N-methylalanine in 200 ml of toluene. The mixture is concentrated and the residue is distilled.

WORKUP

后处理

  1. concentrationThe mixture is concentrated
  2. distillationthe residue is distilled