HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Hydroxyproline → HCID 54239052, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Hydroxyproline | HCID 5810 | — |
| Reactant | Ethyl allyl(2-oxoethyl)carbamate | HCID 11084330 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54239052 | HCID 54239052 | — |
Reaction Steps
8.6 g (50 mmol) of ethyl N-allyl-N-(2-oxoethyl) -carbamate are heated at 120° C. overnight with 6.6 g (50 mmol) of trans-4-hydroxyproline in 200 ml of dimethylformamide. The mixture is concentrated and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05071999 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-d9548029e1d64d3abd8a6a59503991db |
| Source note | uspto-grants-1991_12 |