HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pipecolic Acid → HCID 54122708, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pipecolic Acid | HCID 849 | — |
| Reactant | Ethyl allyl(2-oxoethyl)carbamate | HCID 11084330 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54122708 | HCID 54122708 | — |
Reaction Steps
17.1 g (0.1 mol) of ethyl N-allyl-N-(2-oxoethyl) -carbamate are heated under reflux overnight with 13 g (0.1 mol) of piperidine-2-carboxylic acid in 200 ml of toluene. The mixture is concentrated and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05071999 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-8503c89a0c69450cbba885657400bb40 |
| Source note | uspto-grants-1991_12 |