HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,5-Dimethyl-4-thiazolidinecarboxylic acid → HCID 54322387, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,5-Dimethyl-4-thiazolidinecarboxylic acid | HCID 85822 | — |
| Reactant | Ethyl allyl(2-oxoethyl)carbamate | HCID 11084330 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54322387 | HCID 54322387 | — |
Reaction Steps
8.6 g (50 mmol) of ethyl N-allyl-N-(2-oxoethyl) -carbamate are heated under reflux overnight with 8.1 g (50 mmol) of 5,5-dimethylthiazolidine-4-carboxylic acid in 200 ml of toluene. The mixture is concentrated and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05071999 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-099370b337774a45a13d0be893c78b65 |
| Source note | uspto-grants-1991_12 |