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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1460793Generated: November 2, 2026

Water → HCID 19100948, compound

https://huagongshe.com/reaction/1460793

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
ReactantTolueneHCID 1140—
Reactant2-(Benzylamino)acetic acidHCID 86965—
Reactantethyl N-(but-2-enyl)-N-(2-oxoethyl)-carbamateHCID 53690408—
ProductHCID 19100948HCID 19100948—

Reaction Steps

18.5 g (0.1 mol) of ethyl N-(2-buten-1-yl)-N-(2-oxoethyl)-carbamate are heated under reflux overnight in a water separator with 16.5 g (0.1 mol) of N-benzylglycine in 300 ml of toluene. The mixture is concentrated and the residue is distilled.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05071999
Source datasetuspto-grants-1991_12
ORD IDord-bb0e7863a95b40bead75b2e19976dec8
Source noteuspto-grants-1991_12