Vinyltrichlorosilane → 1,1,1,4,4,4-Hexachloro-1,4-disilabutane

HRID 1460823Notes

Reaction equation

HRID 1460823 reaction equation
[CH:1]([Si:3]([Cl:6])([Cl:5])[Cl:4])=[CH2:2].[Cl:7][SiH:8]([Cl:10])[Cl:9]>>[Cl:4][Si:3]([Cl:6])([Cl:5])[CH2:1][CH2:2][Si:8]([Cl:10])([Cl:9])[Cl:7]

Participants

3

Reactant 2

HCID 6413VinyltrichlorosilaneHCID 24811Trichlorosilane

Product 1

HCID 756311,1,1,4,4,4-Hexachloro-1,4-disilabutaneYield 98%

Procedure

As in Example 1, 53.3 grams (0.33 mol) of vinyltrichlorosilane was reacted with 46.1 grams (0.34 mol) of trichlorosilane to obtain 96.0 grams (yield 98%) of 1,2-bis(trichlorosilyl)ethane.

Sources & evidence

ORD record
ord-80c97804d3c34f6a839cf64a3a503d9b
Source dataset
uspto-grants-1991_12
Patent number
US05072012

Reaction notes

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