Tetrahydrofuran → HCID 67867206, compound

Participants

Reaction Steps

3.5g (15 mmoles) of 3,5-di-t-butylphenylhydrazine and 2.6g (15 mmoles) of methyl 4-formylbenzoate were stirred for 1 hour under reflux in 150ml of a 1:1 mixture of tetrahydrofuran and ethanol. After evaporation of the solvent the residue was digested with ethanol at the boil and then cooled, filtered off in vacuo and rinsed with ethanol. After drying in vacuo at ambient temperature, there were obtained 3.2g of the above compound, m.p. 215°-220° C.

Provenance & Evidence