Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Water | HCID 962 | — |
| Reactant | gamma-Glycidoxypropyltriethoxysilane | HCID 102856 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Glycidoxypropyl Silanol | HCID 123537430 | — |
Reaction Steps
In a three-necked flask equipped with a stirrer, dropping funnel and reflux condenser, 500 g water were adjusted with dilute acetic acid to a pH value of 4 to 4.5. 15 g glycidoxypropyl triethoxysilane were then added dropwise, the mixture being heated to 90° C. This temperature was maintained for 1 hour.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05073588 |
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| Source dataset | uspto-grants-1991_12 |
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| ORD ID | ord-c4d35faa540c401f800b316ffa07cf99 |
|---|
| Source note | uspto-grants-1991_12 |
|---|
