HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → Acetyl chloride, (benzoyloxy)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 12647149 | HCID 12647149 | — |
| Product | Acetyl chloride, (benzoyloxy)- | HCID 10888895 | 88% |
Reaction Steps
A mixture of 2-(benzoyloxy)acetic acid (12.6 g) and thionyl chloride (15 ml) was refluxed for 3 h. Excess of thionyl chloride was removed in vacuo and the crude (benzoyloxy)acetyl chloride obtained was purified by distillation in vacuo. The yield was 88%. Mp 25°-26° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05073641 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-894768fca82143b29a962f66aa2071e8 |
| Source note | uspto-grants-1991_12 |