HRID1461147

反应详情

EQUATION

反应方程式

HRID 1461147 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of methyl 6-dimethylamino-4,4-diphenyl-2-heptenoate (60 mg), 10% Pd/C (10 mg), and methanol was hydrogenated at room temperature for 18 hours. The mixture was filtered through a short pad of celite, and the filtrate was rotary evaporated to give methyl 6-dimethylamino-4,4-diphenyl-heptanoate, as a crude material which was then dried in vacuo.

WORKUP

后处理

  1. filtrationThe mixture was filtered through a short pad of celite
  2. customthe filtrate was rotary evaporated