Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Chromic Acid → 4,4-Diphenylnon-8-en-3-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Chromic Acid | HCID 24425 | — |
| 반응물 | 4,4-Diphenylnon-8-en-3-ol | HCID 19981511 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 4,4-Diphenylnon-8-en-3-one | HCID 19981508 | 78.8% |
반응 단계
One hundred seventy milligrams of 4,4-diphenylnon-8-en-3-ol was dissolved in acetone (10 ml), and then treated with 2.7M chromic acid solution (0.04 ml). After 10 min, the excess oxidant was destroyed with isopropanol, and the mixture was diluted with ether (20 ml). Filtration through a pad of celite and concentration yielded 133 mg of 4,4-diphenylnon-8-en-3-one, as an amorphous white solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05073629 |
| 출처 데이터셋 | uspto-grants-1991_12 |
| ORD ID | ord-ed73cb74f4f64592b7d42a4b31c17767 |
| 출처 메모 | uspto-grants-1991_12 |