HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 19980029, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | N-Methylaniline | HCID 7515 | — |
| Reactant | Ethyl chloroacetate | HCID 7751 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Product | HCID 19980029 | HCID 19980029 | — |
Reaction Steps
A mixture of N-methyl aniline (198 g, 1.85 mol), ethylchloroacetate (227 g, 1.85 mol), potassium carbonate (256 g, 1.85 mol), potassium iodide (15 g, 0.93 mol), and 750 mL of absolute ethanol was stirred at reflux for 72 hours, then cooled and filtered. The solvent was removed from the filtrate at reduced pressure, and the residue was fractionally distilled in vacuo. A slightly yellow oil was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05075043 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-f94a5687b4bd4945a5d43c1ef91f15c6 |
| Source note | uspto-grants-1991_12 |