HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl acetoacetate → HCID 67838630, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl acetoacetate | HCID 7757 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 19980380 | HCID 19980380 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Product | HCID 67838630 | HCID 67838630 | — |
Reaction Steps
0.28 g (9.3 mmol) of 80% strength sodium hydride, 0.97 g (8.4 mmol) of methyl acetoacetate, 8.6 ml (14 mmol) of 15% strength butyllithium and 0.99 g (2.88 mmol) of the compound from Example 27 are reacted analogously to the procedure for Example 7.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05075311 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-bd638d3842054fedad16367899773b52 |
| Source note | uspto-grants-1991_12 |