HCID 22841876, compound → HCID 53932422, compound

Participants

Reaction Steps

A solution of 11 (30 mg) in 2 mL of methanol was hydrogenated in the presence of 5% Pd/C (10 mg) for 24 hours. The reaction was monitored by TLC. The suspension was filtered and, after complete evaporation of the solvent and chromatography, pure methyl 1-O-(11-methoxycarbonylundecyl)-2, 4-di-O-acetyl-β-D-glucopyranosuronate (12) was obtained. The 1H NMR data confirmed the complete debenzylation.

Provenance & Evidence