HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 13532834, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Benzene | HCID 241 | — |
| Reactant | Cyclohept-2-en-1-amine | HCID 11263481 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13532834 | HCID 13532834 | 83.8% |
Reaction Steps
A mixture of 2-cycloheptenylamine (11.1 g, 0.1 mole), benzaldehyde (10.6 g, 0.1 mole) and benzene (50 ml) was heated under reflux, and resulting water was removed by azeotropic distillation. The mixture was concentrated to obtain 16.7 g of N-benzylidene-2-cycloheptenylamine [Compound (280)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05075488 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-2f4485345bfc47c08a9aad07fbd25100 |
| Source note | uspto-grants-1991_12 |