HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene → N-(Cyclohex-2-en-1-yl)cyclohexanimine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene | HCID 241 | — |
| Reactant | Cyclohexanone | HCID 7967 | — |
| Reactant | HCID 10931371 | HCID 10931371 | — |
| Catalyst | Zincchloride | HCID 3007855 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-(Cyclohex-2-en-1-yl)cyclohexanimine | HCID 13272647 | 69.9% |
Reaction Steps
A mixture of 2-cyclohexenylamine (9.7 g, 0.1 mole), cyclohexanone (9.8 g, 0.1 mole), zinc chloride (0.16 g) and benzene (50 ml) was heated under reflux, and resulting water was removed by azeotropic distillation. The mixture was concentrated and distilled to obtain 12.4 g of N-cyclohexylidene-2-cyclohexenylamine [Compound (344)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05075488 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-97d989fe4c36423e9ac8c2d0040265a9 |
| Source note | uspto-grants-1991_12 |