HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 13532852, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Cyclohept-2-en-1-amine | HCID 11263481 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 13532852 | HCID 13532852 | 94.8% |
Reaction Steps
Conc. hydrochloric acid (10.1 g) was added dropwise to a mixture of 2-cycloheptenylamine (11.1 g, 0.1 mole) and isopropyl alcohol (24 g) with stirring and ice-cooling. The reaction mixture was concentrated under reduced pressure, and the deposited crystal was washed with diethyl ether and dried to obtain 14 g of 2-cycloheptenylamine hydrochloride [Compound (349)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05075488 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-979f72f9093e400c9629756724ccec25 |
| Source note | uspto-grants-1991_12 |