Sodium;3-phenylprop-2-enoate → HCID 86745355, compound

Participants

Reaction Steps

A four-necked flask fitted with stirrer and condenser means was charged with 43.3 g of oleyltrihydroxyethylammonium chloride, 20 g of sodium cinnamate and 200 g of isobutyl alcohol and the reaction was conducted at 40°-50° C. in an atmosphere of nitrogen gas introduced at a low flow rate for 6 hours. The precipitate was then collected by filtration and washed with 30 ml of isobutyl alcohol. The filtrate and the washings were combined and concentrated under reduced pressure and the residue was dissolved in 200 g of toluene and filtered. Finally, the filtrate was concentrated to give 50.9 g (theoretical yield 54.5 g) of oleyltrihydroxyethylammonium cinnamate as a waxy product. The elemental analysis is shown below.

Provenance & Evidence