HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 1-Cyclohexyloxy-2,2,6,6-tetramethyl-4-acrylamidopiperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Acryloyl chloride | HCID 13140 | — |
| Reactant | 4-Amino-1-cyclohexyloxy-2,2,6,6-tetramethylpiperidine | HCID 22277984 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1-Cyclohexyloxy-2,2,6,6-tetramethyl-4-acrylamidopiperidine | HCID 19979425 | — |
Reaction Steps
The procedure of Example 3 is repeated using 3.0 grams of 4-amino-1-cyclohexyloxy-2,2,6,6-tetramethylpiperidine, 0.92 ml of acryloyl chloride and 1.8 ml of triethylamine in methylene chloride. The title compound is isolated as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05077340 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-50f76b43fdeb45acbed30df3d9108418 |
| Source note | uspto-grants-1991_12 |