HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 14719550, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | HCID 10802931 | HCID 10802931 | — |
| Product | HCID 14719550 | HCID 14719550 | — |
Reaction Steps
850 mg of 4-(3,4-dimethoxyphenyl)-7-methyl-1,2,3,4-tetrahydroisoquinoline was dissolved in 17 ml of 48% hydrobromic acid, and the mixture was heated under reflux under an argon gas stream for 3 hours. The reaction solution was cooled, and the crystals obtained were collected by filtration, giving 620 mg of 4-(3,4-dihydroxyphenyl)-7-methyl-1,2,3,4-tetrahydroisoquinoline hydrobromide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05077406 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-eb4052733b424eed9b1a83864d50787a |
| Source note | uspto-grants-1991_12 |