HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → HCID 10416740, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 5-Methylthiazole | HCID 137980 | — |
| Reactant | 3-(bromomethyl)phenyl-N-[2-[4-(tetradecyloxy)phenyl]ethyl]acetamide | HCID 86745366 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 10416740 | HCID 10416740 | — |
Reaction Steps
A mixture of 2.5 g N-[3-(bromomethyl)phenyl-N-[2-[4-(tetradecyloxy)phenyl]ethyl]acetamide and 2.28 g of 5-methylthiazole in 50 ml of toluene is refluxed for 5 hours, cooled and ether added. The solid is collected by centrifugation and washed several times with ether then vacuum dried to give 1.8 g of the desired product as a white solid, m.p. 136°-140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05077409 |
| Source dataset | uspto-grants-1991_12 |
| ORD ID | ord-34ad10f92e644bc4a606e473b3e7fabc |
| Source note | uspto-grants-1991_12 |