HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4,6,6-trichloro-3,3-dimethyl-5-hexenoate → 2(3H)-Furanone, 5-(2,2-dichloroethenyl)dihydro-4,4-dimethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4,6,6-trichloro-3,3-dimethyl-5-hexenoate | HCID 3042523 | — |
| Reactant | 5-Hexenoic acid, 4,6,6-trichloro-3,3-dimethyl-, methyl ester | HCID 10999791 | — |
| Product | 2(3H)-Furanone, 5-(2,2-dichloroethenyl)dihydro-4,4-dimethyl- | HCID 10198203 | 95% |
Reaction Steps
The above procedure was repeated except that 27.4 parts of ethyl 3,3-dimethyl-4,6,6-trichloro-5-hexenoate was used in lieu of methyl 3,3-dimethyl-4,6,6-trichloro-5-hexenoate. In this case, 19.8 parts of 3,3-dimethyl-4-(2',2'-dichlorovinyl)-4-butanolide was obtained (yield 95%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04458090 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-6d5d06d8e26949958ffccad40ea74589 |
| Source note | uspto-grants-1984_07 |