HCID 13320312, compound → HCID 13320360, compound

HRID 1462111Notes

Reaction equation

HRID 1462111 reaction equation
[Cl:1]C1C=CC(SC(SC2C=CC(Cl)=CC=2)CN2C=CN=C2)=CC=1.Cl[C:25]1[CH:48]=[CH:47][C:28]([CH2:29][S:30][CH:31]([S:38][CH2:39][C:40]2[CH:45]=[CH:44][C:43]([Cl:46])=[CH:42][CH:41]=2)[CH2:32][N:33]2[CH:37]=[CH:36][N:35]=[CH:34]2)=C[CH:26]=1>>[ClH:1].[Cl:46][C:43]1[CH:42]=[CH:41][C:40]([CH2:39][S:38][CH:31]([S:30][C:29]2[CH:26]=[CH:25][C:48]([Cl:1])=[CH:47][CH:28]=2)[CH2:32][N:33]2[CH:37]=[CH:36][N:35]=[CH:34]2)=[CH:45][CH:44]=1

Participants

3

Reactant 2

HCID 13320312HCID 13320312, compoundHCID 13320314HCID 13320314, compound

Product 1

HCID 13320360HCID 13320360, compoundYield 55%

Procedure

The results of gas-liquid chromatography from a similar experiment showed the crude mixture of free bases to consist of: 3% of 1-[2,2-bis(4-chlorophenylthio)ethyl]-1H -imidazole, 55% of the title compound and 22% of 1-[2,2-bis(4-chlorobenzylthio)ethyl]-1H-imidazole.

Workup

  1. customThe results of gas-liquid chromatography from a similar experiment
  2. additionmixture of free bases

Sources & evidence

ORD record
ord-fae07a3a6f874ecc83884634cc958da4
Source dataset
uspto-grants-1984_07
Patent number
US04458079

Reaction notes

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