HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Imidazolidinone → HCID 20454110, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Imidazolidinone | HCID 8453 | — |
| Reactant | 2H-1,2,4-Oxadiazin-3(4H)-one, dihydro-5-thioxo- | HCID 3006908 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 20454110 | HCID 20454110 | 100.8% |
Reaction Steps
To a solution of 1.0 g (0.0075 mole) of 6H-1,2,4-oxadiazin-3(2H)-one-5(4H)-thione in 50 ml of dry freshly distilled dioxane is added 0.66 g (0.007 mole) of 2-imidazolidone. After stirring at room temperature for 17 hours, the solution is filtered, washed with chloroform and dried to give a yield of 1.3 g (94 percent) of 5-(2-oxo-1-imidazolidinyl)-6H-1,2,4-oxadiazin-3(2H)-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04459403 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-45b23b7e298243139d0e0660baed23a1 |
| Source note | uspto-grants-1984_07 |