HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(2-Aminoethoxy)-2-hydroxybenzamide → 5-[2-(Benzylamino)-ethoxy]-salicylamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(2-Aminoethoxy)-2-hydroxybenzamide | HCID 23049694 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 5-[2-(Benzylamino)-ethoxy]-salicylamide | HCID 13754419 | — |
Reaction Steps
The 5-(2-aminoethoxy)-salicylamide with a melting point of 140°, which is required as a starting material, is obtained analogously to Example 21 by catalytic debenzylation of 5-(2-benzylaminoethoxy)-salicylamide by means of 5% palladium-on-charcoal catalyst in methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460580 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-05b14aa8da234473a71465ebb84223d5 |
| Source note | uspto-grants-1984_07 |