HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → n-Butyl 2-[2-phenyl-5-(3-thienyl)-4-oxazolyl]acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-[2-Phenyl-5-(3-thienyl)-4-oxazolyl]acetic acid | HCID 13105439 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | n-Butyl 2-[2-phenyl-5-(3-thienyl)-4-oxazolyl]acetate | HCID 13105445 | 66.9% |
Reaction Steps
2 g of 2-[2-phenyl-5-(3-thienyl)-4-oxazolyl]acetic acid, 3 g of thionyl chloride and 30 ml of n-butanol are treated in the same manner as described in Example 13. 0.8 g of n-butyl 2-[2-phenyl-5-(3-thienyl)-4-oxazolyl]acetate is thereby obtained. Yield: 33.5%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460596 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-9565d802cdac4216a9022f0c2be7fbdc |
| Source note | uspto-grants-1984_07 |