HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Pentanol → HCID 13105449, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Pentanol | HCID 6276 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 4-Oxazoleacetic acid, 2-(p-fluorophenyl)-5-(3-thienyl)- | HCID 3069787 | — |
| Product | HCID 13105449 | HCID 13105449 | 52.8% |
Reaction Steps
2 g of 2-[2-(4-fluorophenyl)-5-(3-thienyl)-4-oxazolyl]acetic acid, 0.5 g of potassium hydroxide, 4.2 g of oxalyl chloride and 20 ml of n-pentanol are treated in the same manner as described in Example 17. 1.3 g of n-pentyl 2-[2-(4-fluorophenyl)-5-(3-thienyl)-4-oxazolyl]acetate are thereby obtained. Yield: 52.8%
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460596 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-d3b18125ff92431d972207fae2e5a50e |
| Source note | uspto-grants-1984_07 |