HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzoyl chloride → N-(2-chlorobenzoyl)-N-[(3-thienylcarbonyl)methyl]amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzoyl chloride | HCID 69110 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 2-Amino-1-(3-thienyl)ethanone hydrochloride | HCID 13105417 | — |
| Product | N-(2-chlorobenzoyl)-N-[(3-thienylcarbonyl)methyl]amine | HCID 13105429 | 95.8% |
Reaction Steps
7.5 g of N-[(3-thienylcarbonyl)methyl]amine hydrochloride, 10.0 g of sodium bicarbonate and 8.86 g of 2-chlorobenzoyl chloride are treated in the same manner as described in Preparation 1-(3). 11.3 g of N-(2-chlorobenzoyl)-N-[(3-thienylcarbonyl)methyl]amine are thereby obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460596 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-cac61d1bc9be4d44848ea940bb8d0e6b |
| Source note | uspto-grants-1984_07 |