HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53693383, compound → HCID 13102421, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53693383 | HCID 53693383 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 13102421 | HCID 13102421 | 71.6% |
Reaction Steps
4.44 g (20 mmols) of 1-chloro-3,3-dimethyl-2-phenoxy-1,4-pentadiene are warmed to 100° C. in 20 ml of dioxane and 10 ml of 50% sulphuric acid, during the course of 6 hours. The working-up according to Example B1(a) yields 2.1 g of 1-chloro-3,3-dimethyl-pent-4-en-2-one, which are 72% of theory.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04460793 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-2e9d3eed60ec46b6a6fad0a3869a05df |
| Source note | uspto-grants-1984_07 |