HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → Bicyclo(2.2.1)hept-1-yl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 2-Norbornene | HCID 10352 | — |
| Product | Bicyclo(2.2.1)hept-1-yl acetate | HCID 13351884 | 95% |
Reaction Steps
To illustrate reaction of a cycloolefin in the process, a mixture of norbornene (bicyclo[2.2.1]-2-heptene) and acetic acid was reacted over HZSM-12 zeolite. The reaction was carried out on a steam bath at about 100° C. for 5.5 hours. The addition product, norbornyl acetate, was formed in about 95% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04461729 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-389226bb969841a698c1a2375dea84a9 |
| Source note | uspto-grants-1984_07 |