HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1462996Generated: November 1, 2026
Dimethyl Sulfate → 4-Methyl-4-(2-{[4-(pyren-1-yl)butanoyl]oxy}ethyl)morpholin-4-ium methyl sulfate
https://huagongshe.com/reaction/1462996
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | 2-(Morpholin-4-yl)ethyl 4-(pyren-1-yl)butanoate | HCID 20450718 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 4-Methyl-4-(2-{[4-(pyren-1-yl)butanoyl]oxy}ethyl)morpholin-4-ium methyl sulfate | HCID 20026233 | — |
Reaction Steps
Dimethyl sulfate (6 mls; 0.063M) is added dropwise to a solution of 4-[2-[1-oxo-4-(1-pyrenyl)butoxy]ethyl]morpholine (2.64 grams; 0.006M) in dry acetone (50 mls) at 0° C., and the resulting reaction mixture is then heated at 50° C. for 1.5 hours. The reaction mixture is cooled to ambient temperature and filtered to recover a precipitate of the desired compound which weighs 2.28 grams, after drying in a vacuum oven, and melts at 115°-117° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04462931 |
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| Source dataset | uspto-grants-1984_07 |
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| ORD ID | ord-98a099d2f6044d4683e3bb4952e7924c |
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| Source note | uspto-grants-1984_07 |
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