HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(L-alanyl)-4-(S)-(phenylthio)-L-proline, phenylmethyl ester → 1-(L-alanyl)-4-(S)-(phenylthio)-L-proline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(L-alanyl)-4-(S)-(phenylthio)-L-proline, phenylmethyl ester | HCID 131713593 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(L-alanyl)-4-(S)-(phenylthio)-L-proline | HCID 22827196 | — |
Reaction Steps
To a solution of 5.0 grams of 1-(L-alanyl)-4-(S)-(phenylthio)-L-proline, phenylmethyl ester in 200 ml. of aqueous ethanol there is added 1 gram of freshly prepared palladium black and the mixture is hydrogenated at 50 psi of hydrogen. The reaction mixture is filtered and concentrated under reduced pressure to yield the desired (S)-1-(L-alanyl)-4-(phenylthio)-L-proline.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04462943 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-7315f6cee2224c87ae076bcdf66b5c50 |
| Source note | uspto-grants-1984_07 |