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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1463038Generated: November 1, 2026

Sodium Methoxide → HCID 11791428, compound

https://huagongshe.com/reaction/1463038

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium MethoxideHCID 10942334—
ReactantHCID 11192185HCID 11192185—
ProductHCID 11791428HCID 1179142854.6%

Reaction Conditions

Temperature0 °C

Reaction Steps

1-(2',3',5'-tri-O-benzoyl-β-D-arabinofuranosyl)-2-nitroimidazole (150 mg, 0.27 mmol) was added to 2.5 ml of 0.025 M methanolic sodium methoxide. The mixture was stirred at 0° C. for three hours and then purified by preparative TLC using chloroform:methanol (6:1) to give 36 mg (54.6%) of the title product as white needles, mp 172° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04462992
Source datasetuspto-grants-1984_07
ORD IDord-6d87b9a37e5a4e33a217f3a10c083ede
Source noteuspto-grants-1984_07