Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Reactant | HCID 11192185 | HCID 11192185 | — |
| Product | HCID 11791428 | HCID 11791428 | 54.6% |
Reaction Steps
1-(2',3',5'-tri-O-benzoyl-β-D-arabinofuranosyl)-2-nitroimidazole (150 mg, 0.27 mmol) was added to 2.5 ml of 0.025 M methanolic sodium methoxide. The mixture was stirred at 0° C. for three hours and then purified by preparative TLC using chloroform:methanol (6:1) to give 36 mg (54.6%) of the title product as white needles, mp 172° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04462992 |
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| Source dataset | uspto-grants-1984_07 |
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| ORD ID | ord-6d87b9a37e5a4e33a217f3a10c083ede |
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| Source note | uspto-grants-1984_07 |
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