HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → HCID 13191666, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 13191644 | HCID 13191644 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13191666 | HCID 13191666 | — |
Reaction Steps
1.1 g of NaHCO3 were added to 3.5 g (0.012 mole) of ethyl 6-propyl-1,2,4-triazolo[1,5-c]quinazolin-5-one-2-carboxylate in 50 ml of water, and the mixture was refluxed for 8 hours. It was then filtered, and acidified with dilute HCl, and the precipitate was filtered off under suction and dried. Yield: 1.0 g (32%), mp. 233°-235° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04463007 |
| Source dataset | uspto-grants-1984_07 |
| ORD ID | ord-ba8cf7d4027648de91cd8e5705e59acc |
| Source note | uspto-grants-1984_07 |