HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylonitrile → HCID 10420903, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 19090901 | HCID 19090901 | — |
| Product | HCID 10420903 | HCID 10420903 | — |
Reaction Steps
To 15.7 g of t-butylphosphonous acid-isopropylester in 6.3 ml of acrylonitrile are added 21 ml of sodium isopropylate (0.25 molar). After the exothermic reaction (the temperature rises to 100°) the suspension is filtered, the filtrate evaporated and the residue distillated to yield isopropyl 2-cyanoethyl(t-butyl)phosphinate as an oil, b.p. 121°/8 Pa, nD20 =1.4480.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05300679 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-9a5bcc7e9e1f40a88b422e5e64d21048 |
| Source note | uspto-grants-1994_04 |