HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 86746431, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 15296097 | HCID 15296097 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86746431 | HCID 86746431 | — |
Reaction Steps
To a solution of 1,1-bis(4-pyridinylmethyl)-3-phenyl-1H-indene (1.0 g, 2.7 mmol) in dichloromethane was added methanesulfonic acid (5.4 mmol, 0.52 g, 0.35 ml). The solvent was evaporated and the residue was recrystallized from ethyl acetate/ispropanol to give white crystals, 0.8 g, m.p. >250° .
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05300642 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-65405acbd0fc42969d2e39daec58ef82 |
| Source note | uspto-grants-1994_04 |