HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → 1-Azaphenanthrene-5,6-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Benzo(F)Quinoline | HCID 6796 | — |
| Reactant | Iodine pentoxide | HCID 159402 | — |
| Product | 1-Azaphenanthrene-5,6-dione | HCID 19922456 | — |
Reaction Steps
Following the procedure described in Example 608, Part A, 37.5 g (0.153 mole) of commercial 1-azaphenanthrene, 55 g (0.165 mole) of iodine pentoxide in 600 ml glacial acetic acid were refluxed 2 hours. Identical workup yielded 8.4 g, m.p. 215°-16°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05300642 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-512e2134ed654d059f3f6d156789530c |
| Source note | uspto-grants-1994_04 |