Sodium styrenesulfonate → HCID 86747742, compound

HRID 1463730Notes

Reaction equation

HRID 1463730 reaction equation
[Br-].[CH2:2]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][NH+:17]([CH3:19])[CH3:18])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[CH:20]([S:28]([O-:31])(=[O:30])=[O:29])=[CH:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1.[Na+]>O>[CH:20]([S:28]([O-:31])(=[O:29])=[O:30])=[CH:21][C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1.[CH2:2]([CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][NH+:17]([CH3:19])[CH3:18])[C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1

Participants

4

Reactant 2

HCID 53627496Sodium styrenesulfonateHCID 67744700HCID 67744700, compound

Product 1

HCID 86747742HCID 86747742, compoundYield 81%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Benzyloctyldimethylammonium bromide as a 50 weight % ethanolic solution (183 ml) was added to a solution of sodium styrenesulphonate (50 g) in water. The resulting dense white precipitate was collected by filtration, washed with water, dried and recrystallised from toluene to give benzyloctyldimethylammonium styrenesulphonate (85 g, 81%) MONOMER 3.

Workup

  1. filtrationThe resulting dense white precipitate was collected by filtration
  2. washwashed with water
  3. customdried
  4. customrecrystallised from toluene

Sources & evidence

ORD record
ord-81a6665410ba40cbb205e8ee9a7a30d1
Source dataset
uspto-grants-1994_04
Patent number
US05302192

Reaction notes

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