Hydrazine → HCID 21554741, compound

HRID 1463813Notes

Reaction equation

HRID 1463813 reaction equation
[NH2:1]N.[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11]C1C=CC=C2C(NC(=O)C=12)=O>CO>[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][NH2:1]

Participants

4

Reactant 2

HCID 9321HydrazineHCID 544460722-(N-methylpiperazinyl)ethylphthalimide

Product 1

HCID 21554741HCID 21554741, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 2-(N-methylpiperazinyl)ethylphthalimide (218 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

Workup

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

Sources & evidence

ORD record
ord-d00738842f674f47beb9d1a326135ce1
Source dataset
uspto-grants-1994_04
Patent number
US05302593

Reaction notes

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