Hydrazine → HCID 54275604, compound

HRID 1463817Notes

Reaction equation

HRID 1463817 reaction equation
[NH2:1]N.[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12][CH2:13]C1C=CC=C2C(NC(=O)C=12)=O>CO>[CH3:3][N:4]1[CH2:9][CH2:8][NH:7][CH2:6][CH:5]1[CH2:10][CH2:11][CH2:12][CH2:13][NH2:1]

Participants

4

Reactant 2

HCID 9321HydrazineHCID 538263884-(N-methylpiperazinyl)butylphthalimide

Product 1

HCID 54275604HCID 54275604, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Hydrazine (aqueous solution at 35% by wt.) (0.15 ml; 1.6 mmoles) was added to 4-(N-methylpiperazinyl)butylphthalimide (240 mg; 0.8 mmoles) in methanol (5 ml) and the resulting solution was refluxed. Reaction times and process as per Example 1.

Workup

  1. temperaturethe resulting solution was refluxed
  2. customReaction times and process as per Example 1

Sources & evidence

ORD record
ord-8fe237a629f34fea9a2a27849c8afeba
Source dataset
uspto-grants-1994_04
Patent number
US05302593

Reaction notes

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