HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dimethyl-2-imidazolidinone → HCID 54173339, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dimethyl-2-imidazolidinone | HCID 6661 | — |
| Reactant | 2-Aminobiphenyl | HCID 7015 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 54173339 | HCID 54173339 | — |
Reaction Steps
A mixture of 1,3-dimethyl-2-imidazolidinone (5.5 g) in benzene (30 ml), 2-aminobiphenyl (5.1 g) in benzene (20 ml) and phosphorus oxychloride (4.4 ml) was heated at 80°-85° C. for 20 hours to yield 2-(1,3-dimethyl-2-imidazolidinylideneamino)biphenyl (m.p. 90°-91° C.) which was recrystallised from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05302720 |
| Source dataset | uspto-grants-1994_04 |
| ORD ID | ord-9e551a85993d4893a2107b753f26be9c |
| Source note | uspto-grants-1994_04 |